Knowledge Base

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View3
  • IRMS
  • EA IsoLink
  • Isotope Fingerprints
  • Tomatoes
  • Organic Vegetables

EA-IRMS: Detecting organic grown vegetables

Christopher Brodie and Oliver Kracht

Thermo Fisher Scientific, Bremen, Germany

AB30399

Goal: In this application brief we show nitrogen isotope measurements on tomato samples and are able to conclude which tomatoes were grown using organic fertilizers and which tomatoes were grown using synthetic fertilizers.

View4
  • IRMS
  • EA IsoLink
  • Isotope Fingerprints
  • Cosmetics
  • Shark Liver Oil
  • Olive Oil

EA-IRMS: Detection of squalane from animal and vegetable sources

Sylvie Guibert (1), Magali Batteau (1), Patrick Jame (1) and Christopher Brodie (2)

1) Univ Lyon, CNRS, Université Claude Bernard Lyon 1, ENS de Lyon, Institut des Sciences Analytiques, Villeurbanne, France; 2) Thermo Fisher Scientific, Bremen, Germany

AB30276

Goal: This application brief shows that the carbon isotope fingerprint of cosmetics can be used for product labeling fraud.

View4
  • IRMS
  • Stable Isotopes
  • Forensics

Forensic Applications of Isotope Ratio Mass Spectrometry

Lesley A. Chesson

IsoForensics Inc.

Spectroscopy Online

Goal: This manuscript discusses the application of two common instrument configurations used for gas source IRMS - dual inlet IRMS and continusou flow IRMS - and how they are useful in the field of forensic science.

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  • MC-ICPMS
  • Neptune Plus
  • High Resolution ICP-MS
  • Element 2/XR
  • Gas Chromatography
  • Speciation
  • GC Transferline

Thermo Scientific GCI Series Interface

Thermo Fisher Scientific, Bremen, Germany

PS43370

Goal: The Thermo Scientific™ GCI Series Interface is a range of products that spans the full Thermo Scientific™ ICP-MS portfolio. The GC transferline that is key part of this kit is highly flexible and lightweigthed and enables improved chromatographic separation for high boiling compounds.

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  • IRIS
  • Delta Ray
  • CO2
  • Carbon and Oxygen Isotopes

The power of stable isotope analysis

HJ Jost

Thermo Fisher Scientific, Bremen, Germany

Spectroscopy Online

Goal: Identifying the origin of CO2 in various samples is a major challenge for environmental scientists, regulators and the industry. Different emission sources create CO2 with different isotopic signatures. The Delta Ray Isotope Ratio Infrared Specometer is a powerful instrument for field CO2 monitoring and analysis.

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  • IRIS
  • Delta Ray
  • CO2
  • Carbon and Oxygen Isotopes

The Delta Ray Road Trip

HJ Jost

Thermo Fisher Scientific, Bremen, Germany

Spectroscopy Online

Goal: The capabilities and robustness of the Delta Ray Isotope Ratio Infrared Spectrometer are demonstrated by installing it in a reacreational vehicle for a road trip across Canada, measuring CO2 concentration and isotope ratios while traveling from coast to coast. 

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  • TIMS
  • Triton Plus

Triton Plus Instrument Poster

Thermo Fisher Scientific, Bremen, Germany

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  • MC-ICPMS
  • Neptune Plus

Neptune Plus Instrument Poster

Thermo Fisher Scientific, Bremen, Germany

View4
  • IRMS
  • Delta V
  • Stable Isotopes
  • Strawberry
  • Essential Oils

Headspace-solid phase microextraction coupled to gas chromatography–combustion-isotope ratio mass spectrometer and to enantioselective gas chromatography for strawberry flavoured food quality control

Luisa Schipilliti (1), Paola Dugo (1,2), Ivana Bonaccorsi (1) and Luigi Mondello (1,2)

1) Dipartimento Farmaco-chimico, Facoltà di Farmacia, Università di Messina, Viale Annunziata, 98168 Messina, Italy, 2) Università Campus-Biomedico, Via A. del Portillo 21, 00128 Roma, Italy

Journal of Chromatography A (2011), V1218 (42), p7481-7486, doi: 10.1016/j.chroma.2011.07.072

Goal: Authenticity assessment of flavoured strawberry foods was performed using headspace-solid phase microextraction (HS-SPME) coupled to gas chromatography–combustion-isotope ratio mass spectrometry (GC–C-IRMS).

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  • IRMS
  • Delta V
  • Stable Isotopes
  • Essential Oils

Evaluation of Gas Chromatography−Combustion−Isotope RatioMass Spectrometry (GC-C-IRMS) for the Quality Assessment of Citrus Liqueurs

Luisa Schipilliti (1), Ivana Bonaccorsi 1), Antonella Cotroneo (1), Paola Dugo (1,2 and Luigi Mondello (1,2)

1) Diaprtimento di Scienze del Farmaco e dei Prodotti per la Salute, Università di Messina, Viale Annunziata, 98168 Messina, Italy, 2) Campus-Biomedico, Via A. del Portillo 21, 00128 Roma, Italy

Journal of Agricultural and Food Chemistry (2013), V61 (8), pp1661–1670, doi: 10.1021/jf3028073

Goal: The aim of this study is to investigate the authenticity of Italian liqueurs, of lemon, bergamot, and mandarin (locally known as “limoncello”, “bargamino”, and “mandarinetto”), comparing the carbon isotope ratios with values determined in genuine cold-pressed peel oils.

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  • IRMS
  • Delta V
  • Stable Isotopes
  • Essential Oils

Genuineness assessment of mandarin essential oils employing gas chromatography-combustion-isotope ratio MS (GC-C-IRMS)

Luisa Schipilliti (1), Peter Quinto Tranchida (1), Danilo Sciarrone (1), Marina Russo (1), Paola Dugo (1), Giovanni Dugo (1), Luigi Mondello (1,2)

1) Dipartimento Farmaco-chimico, Facoltà di Farmacia, Università di Messina, Messina, Italy, 2) Campus Biomedico, Roma, Italy

Goal: Reconstituted mandarin oils are easy to find on the market; useful information on essential oil authenticity, quality, extraction technique, geographic origin and biogenesis can be attained through high-resolution GC of the volatile fraction, or enantioselective GC, using different chiral stationary phases. 

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  • IRMS
  • Delta XL
  • TC/EA
  • Hydrogen Isotopes
  • Essential Oils

Authenticity assessment of lavender oils using GC-P-IRMS: 2H/1H isotope ratios of linalool and linalyl acetate

Steffi Bilke and Armin Mosandl

Institut für Lebensmittelchemie, Biozentrum J.W. Goethe-Universität, Frankfurt/Main, Germany

European Food Research and Technology (2002), V214 (6),  pp532–535, doi: 10.1007/s00217-002-0508-z

Goal: Gas chromatography-pyrolysis-isotope mass spectrometry (GC-P-IRMS) is applied to the authenticity assessment of lavender oils. 

View6
  • IRMS
  • 253 Plus
  • LIDI Software
  • Clumped Isotopes

Carbonate clumped isotope analyses with the long-integration dual-inlet (LIDI) workflow: scratching at the lower sample weight boundaries

Inigo A. Müller (1), Alvaro Fernandez (1), Jens Radke (2), Joep van Dijk (1), Devon Bowen (3), Johannes Schwieters (2) and Stefano M. Bernasconi (1)

1) Geological Institute, ETH Zürich, Switzerland, 2) Thermo Fisher Scientific, Bremen, Germany, 3) Ziggurat GmbH, Stäfa, Switzerland

Rapid Communications in Mass Spectrometry (2017) , V31 (12), pp1057–1066, doi: 10.1002/rcm.7878

Goal: Clumped isotope analyses (Δ47) of carbonates by dual inlet (DI) mass spectrometry require long integration times to reach the necessary high precision due to the low abundance of the rare isotopologue 13C18O16O. We tested an improved analytical workflow that significantly reduces the sample sizes and total analysis time per sample while preserving precision and accuracy.

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  • MC-ICPMS
  • Neptune Plus
  • Mo, Pt isotopes
  • Jupiter

Age of Jupiter inferred from the distinct genetics and  formation times of meteorites 

Thomas S. Kruijer (1, 2), Christoph Burkhardt (1), Gerrit Budde (1) and Thorsten Kleine (1)

1) Institut für Planetologie, University of Münster, Germany, 2) Nuclear and Chemical Sciences Division, Lawrence Livermore National Laboratory, Livermore, USA

Proceedings of the National Academy of Science of the United States of America (2017), V114 (26), pp6712–6716, doi: 10.1073/pnas.1704461114

Goal: Here, using molybdenum and tungsten isotope measurements on iron meteorites, we demonstrate that meteorites derive from two genetically distinct nebular reservoirs that coexisted and remained spatially separated between ∼1 My and ∼3–4 My after Solar System formation. 

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  • TIMS
  • Triton Plus
  • Ca Isotopes

Advances in high precision Ca isotope ratio measurements using TIMS

Claudia Bouman, Dietmar Tuttas, Michael Deerberg and Johannes Schwieters

Thermo Fisher Scientific, Bremen, Germany

Goal: Here we present different measurement strategies for Ca isotope analysis. We discuss pros and cons and examine the ability to measure all Ca isotopes simultaneously (40Ca up to 48Ca) on the TRITON Plus mass spectrometer.