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High-precision in situ analysis of Pb isotopes in glasses using 1013 ohm resistor high gain amplifiers with ultraviolet femtosecond laser ablation multiple Faraday collector inductively coupled plasma mass spectrometry
Jun-Ichi Kimura (1), Qing Chang (1), Nobuyuki Kanazawa (2), Satoshi Sasaki (2) and Bogdan Stefanov Vaglarov (1)
1) Department of Solid Earth Geochemistry, Japan Agency for Marine-Earth Science and Technology (JAMSTEC), 2-15 Natsushima-Cho, Yokosuka 237-0061, Japan, 2) ThermoFisher Scientific Japan, 3-9 Moriya-Cho, Yokohama 221-0022, Japan
Journal of Analytical Atomic Spectrometry (2015), V31, pp790-800, DOI: 10.1039/c5ja00374a
Goal: This paper reports high-precision in situ determination of Pb isotope ratios in glass samples, using 200 nm UV fs laser ablation coupled with the Thermo Scientific Neptune Plus Multicollector ICPMS equipped with 1013 ohm resistor high gain Faraday amplifiers. It present a very elegent algorithm to compensate for the different amplifier responses.
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- TIMS
- Triton Plus
- 1013 ohm amplifiers
- Sr, Nd
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Measurement of small ion beams by Thermal Ionisation Mass Spectrometry using new 1013 Ohm resistors
Koornneef JM (1), Bouman C (2), Schwieters JB (2), Davies GR (3)
1) Faculty of Earth and Life Sciences, Vrije Universiteit Amsterdam, de Boelelaan 1085, 1081HV Amsterdam, The Netherlands, 2) Thermo Fisher Scientific, Hanna-Kunath-Str. 11, Bremen, 28199, Germany, 3) Faculty of Earth and Life Sciences, Vrije Universiteit Amsterdam, de Boelelaan 1085, 1081HV Amsterdam, The Netherlands
Analytica Chimica Acta (2014), V819, pp49–55, DOI:10.1016/j.aca.2014.02.007
Goal: We tested 5 newly manufactured 1013 ohm resistors in the feedback loop of Faraday cup amplifiers to measure small ion beams by Thermal Ionisation Mass Spectrometry (TIMS). To investigate the precision and accuracy of analyses using these new amplifiers we measured Sr and Nd isotopes of reference standards at a range of ion currents (3.2 × 10−16 to 1 × 10−12 A, corresponding to intensities of 32 μV to 100 mV on a default 1011 ohm amplifier) and on small amounts of material (100 and 10 pg).
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Utilize 1013 ohm Amplifier Technology for Multicollector ICPMS
Thermo Fisher Scientific, Bremen, Germany
Goal: This presentation shows new tools for new science: 1013 ohm amplifier technology for achieving higher isotope ratio precision for limited sample amounts and minor isotopes using NEPTUNE Plus
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- TIMS
- Triton Plus
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Utilize 1013 ohm Amplifier Technology for TIMS: U-Pb dating
Thermo Fisher Scientific, Bremen, Germany
Goal: This presentation shows new tools for new science: 1013 ohm amplifier technology adds to U-Pb dating tools
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- TIMS
- Triton Plus
- 1013 ohm amplifiers
- U-Pb
- Zircons
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Use of new 1013 ohm current amplifiers in U and Pb isotope ratio analysis by TIMS
Claudia Bouman, Anne Trinquier, Nicholas Lloyd and Johannes Schwieters
Thermo Fisher Scientific, Bremen, Germany
Goal: In this presentation, we present our latest developments on low noise Faraday cup amplifier technology, that completely avoids the dead time calibration as well as instrumental mass bias effects introduced by ion counters. This technology is ideally suited for high precise U-Pb age dating by ID-TIMS.
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- MC-ICPMS
- TIMS
- High-Resolution ICPMS
- Geochronology
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Multicollector Mass Spectrometry - Geochronology
C. Bouman
Thermo Fisher Scientific, Bremen, Germany
Goal: This presentation describes the technology of multicollector mass spectrometry for the analysis of isotope ratios and explains how the Thermo Scientific product portfolio is ideally suited for geochronology applications
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High Mass Resolution Isotope Ratio Measurements of Iron
S. Weyer (1), J. Schwieters (2) and G. Jung (2)
1) Goethe-Universität Frankfurt am Main, Institut für Geowissenschaften, Germany, 2) Thermo Fisher Scientific, Bremen, Germany
Goal: Here we present a technique of measuring all Fe isotopes simultaneously with high mass resolution, a very effective way to eliminate molecular interferences. Various Fe standards, spiked standards and geological samples were measured with the Thermo Scientific NEPTUNE Multicollector ICP-MS with both, a proprietary Stable Introduction System (SIS) and a desolvating nebulizer (CETAC Aridus) to evaluate the use of static multicollection with high mass resolution.
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- Triton Plus
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- Isotopic Fingerprinting
- S, Ca, Fe, Cu, Sr
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Multicollector ICPMS and TIMS as Tool for Isotopic Fingerprinting
C. Bouman, J.B. Schwieters, N. Lloyd and A. Trinquier
Thermo Fisher Scientific, Bremen, Germany
Goal: Here we describe a selection of applications on isotopic fingerprinting using non-traditional stable isotope systems of S, Ca, Fe, Cu and Sr measured on the Thermo Scientific TRITON Plus and NEPTUNE Plus mass spectrometers
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- TIMS
- Triton Plus
- 1013 ohm amplifiers
- Gain Calibration
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Gain Calibration Protocol for 1013 ohm Resistor Current Amplifiers using the Certified Neodymium Standard JNdi-1 on the TRITON Plus
Anne Trinquier,
Thermo Fisher Scientific, Bremen, Germany
TN30285
Goal: The present technical note presents a gain calibration protocol for 1013 ohm resistor current amplifiers using the certified neodymium standard JNdi-1 on the Thermo Scientific™ TRITON Plus™ Thermal Ionization MS (TIMS).
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1012 ohm Amplifiers for High Precision Isotope Ratio Measurements of Small Sample Sizes
Anne Trinquier, Claudia Bouman, Johannes Schwieters and Nicholas Lloyd
Thermo Fisher Scientific, Bremen, Germany
TN30249
Goal: This technical note is intended to give recommendations on how to use the Tera-Ohm feedback resistors (1012 ohm) amplifiers for small samples and test their performance on the Triton Plus. Major focus is put on noise and decay characteristics.
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- TIMS
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TRITON Plus Thermal Ionization MS Brochure
Thermo Fisher Scientific, Bremen, Germany
BR30240
Goal: Based on more than 35 years of experience in variable multicollector instrumentation, we have developed the Thermo Scientific TRITON Plus, our latest generation Thermal Ionization Mass Spectrometer (TIMS). It combines new, innovative features, like dual RPQ and compact discrete dynode multi ion counting multipliers, with the field-proven technology of the Thermo Scientific TRITON instrument.
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- Neptune Plus
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NEPTUNE Plus Multicollector ICPMS Brochure
Thermo Fisher Scientific, Bremen, Germany
BR30197
Goal: Based on more than 35 years of experience in variable multicollector instrumentation, we have developed the advanced Thermo Scientific NEPTUNE Plus, our latest generation Multicollector ICP Mass Spectrometer. It combines new, innovative features, like dual RPQ, compact discrete dynode multi ion counting multipliers and unmatched sensitivity using the Jet Interface, with the field-proven technology of the NEPTUNE instrument.
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- MC-ICPMS
- Neptune Plus
- S isotopes
- Human Sersum
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Sulfur Isotope Measurement in Human Serum
Emmanuelle Albalat, Philippe Telouk and Francis Albarède
ENS, Lyon, France
AN30300
Goal: The present note describes a method allowing for precise and accurate sulfur isotope measurements on small aliquots of human serum and plasma. This method can also be applied to a broad range of biological samples, such as whole blood, urine or organs. The measurements were done on a Thermo Scientific Neptune Plus Multicollector ICP-MS .
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- Neptune Plus
- Element XR
- Lu-Hf
- U-Pb
- LASS
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Laser Ablation Split Stream (“LASS”) between High Sensitivity SC- and MC-ICP-MS Instruments
N.S. Lloyd (1), T. Lindemann (1), C. Bouman (1) and C.M. Fisher (2)
1) Thermo Fisher Scientific, Bremen, Germany, 2) School of the Environment, Washington State University, Pullman, WA, USA
AN30298
Goal: Thi goal of this study is to demonstrate that simultaneous acquisition of U-Pb age and Hf isotopic composition is possible with small ablation spots (30 μm diameter) using the LASS technique with high-sensitivity ICP-MS instruments
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New Design 1013 ohm Amplifiers for Measurement of Small Ion Beam Currents
Claudia Bouman (1), Anne Trinquier (1), Nicholas Lloyd (1), Johannes Schwieters (1), Janne Koornneef (2) and Gareth Davies (2)
1) VU University, Amsterdam, The Netherlands, 2) Thermo Fisher Scientific, Bremen, Germany
AN30282
Goal: Here we present newly developed amplifiers equipped with 1013 ohm feedback resistors for the Thermo Scientific™ Triton Plus™ TIMS, Neptune Plus™ MC-ICP-MS and Noble Gas product line. A revolutionary new current amplifier design compensates for settling time effects observed with high-gain current amplifiers using high ohmic resistors in the feedback loop.